RUMBLORRRR the unfermentable stuck wash

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RUMBLORRRR the unfermentable stuck wash

Postby nuddy » Thu Jul 26, 2018 8:09 pm

Gday AD's

I've got a bad case of unfermentable rum wash.

The wash in question is now 11 days old and has barely drop a single SG point.

I've tried an vast array of techniques and experiments to get the damm thing chugging along, all to no avail. Let me run you through this character building 11 days.

15/7/18: The1st generation of a wild yeast rum experiment had just finished fermenting and been put through the still so naturally I got stuck into creating the wash for the 2nd gen.

In a 60L fermenting vessel the following was added:
9kg of bundy refinery molasses (ferm sugars of 5kg) was added with
2kg raw sugar
Onto this 6.5L of hot dunder from the 1st generation was added and mixed thoroughly with a stainless steel mash paddle.
4g DAP and 4.1g Fermaid A added along with hot and cold tap water to get it to 34L mark. I don't remember the temperature at this point but I think it was around the 35 C-40 C range.
8L of cold tap water mixed with the yeast trub/bed from gen 1 was then added and mixed thoroughly.

Starting figures for start ya bastard rum.
Temp corrected S.G: 1.100
temp: 30.0 C
pH 5.6

This was temp controlled to 30.0 C by an aquarium heater running off an ink bird controller with the temp probe strapped to the outside of the fermenter buried under a sacrificed stubbie holder to insulate it. 2 layers of towels were wrapped around fermenter to insulate.

16/7/18 - 24hrs later no airlock activity, opened lid no visible signs of fermenting taking hold, pH 4.5, 3 heaped tsp of calcium carbonate added to bump pH back up.
50ml of gen 1 wild yeast slurry warmed slowly in a bain marie style bath of warm water to 28.6 C then pitched into fermenter.

17/7/18 - 24hrs laters, ferm temp 29.2 C, veryyy slow airlock activity 1 bubble every 1-2 mins,

18/7/18- 24hrs laters measurements taken, temp corrected S.G 1.098, temp 26.7 C, pH 4.1
2L was drawn off fermenter and diluted to 3.27L in a 5L demijohn for a S.G of 1.060 to see if lowering S.G would relieve osmotic pressure of yeast and fire up fermentation.

21/7/18- 72hrs later, 80g of dried bakers yeast pitched into now 40L of rum wash.
3.27L lower S.G experiment was heated slowly over stove, had 8g of bakers yeast hydrated and pitched into it along with 2 tsp of calcium carbonate, pH was raised to 4.4, temp 33.0C, SG 1.059

22/7/18- 24hrs later, 40L wash measurements taken, pH 4.1, S.G 1.090, temp 22.0C, 7 tsp calcium carbonate added, then whole wash was diluted with 8.2L filtered tap water to S.G of 1.076, temp 26.0 C, additional bakers yeast pitched onto surface of wash.
3.27L experiment slowly chugging away.

24/7/18- 48hrs later, now 48.2L rum wash now, pH 4.0, temp 28.0C at bottom of wash, 32.0C at surface of wash, S.G 1.070.
3.27L experiment, pH 4.3, temp 18.0C, S.G 1.030, finalllllly somethings fermenting. I then dumped this 3.27L of actively fermenting wash back into the 48.2L of non fermenting rum wash to try get it kicking over.

25/7/18 - 24hrs later, no ferment taken hold, 20g bakers yeast hydrated in warm water with 3 tsp sugar for 25mins, bakers yeast went nuts and was added to approx 52L unfermenting rum wash.

26/7/18 - 24hrs later, S.G 1.070, not moved a single S.G.

I'm at a loss as to why this dammmm wash wont ferment out.

It's got 24hrs before I dump it. Anyone got any ideas on whats going on?
nuddy
 
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Re: RUMBLORRRR the unfermentable stuck wash

Postby coffe addict » Fri Jul 27, 2018 9:03 am

The only times I've had rum wash issues I've changed molasses supplier's and the issue went away.
That said I've no idea what molasses I get as it's always stock feed.
Good luck

Edit: your sg isn't the issue as I've had sg of 1.30 finish with out problems back when I bothered to check
Last edited by coffe addict on Fri Jul 27, 2018 9:05 am, edited 1 time in total.
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Re: RUMBLORRRR the unfermentable stuck wash

Postby nuddy » Fri Jul 27, 2018 6:20 pm

Yeah its got me boggled. Bundy refinery molasses has never steered me wrong.

My brewer roommate has offer a suggestion that since I use tap water unfiltered I may have filled during a chlorine/chloramine spike on the municipal system.

Who knows, this lots going to the drain.
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Re: RUMBLORRRR the unfermentable stuck wash

Postby woodduck » Fri Jul 27, 2018 7:00 pm

I'd love to be able to help but I've got no idea sorry.

This probably won't make you feel better but I had a 200ltr bwko fermenting in the shed with some plastic wrap on it. I went in there the other day and obviously something had jumped on top of it, torn through the plastic and had a bit of a swim around, I'm looking squarely at the pet goat! It looked all funky and pussy and I thought well that will be going out. Went in there today (a week later, yes I'm a lasy bastard) to get rid of it and the bloody thing is bubbling away with a nice crust on it, still no plastic cover :laughing-rolling: so I threw a lid on it and I'll call it goats juice :laughing-rolling: it's funny how ferments can be so unpredictable. I could lend you the goat if you like? :teasing-tease: :laughing-rolling: :laughing-rolling:
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Re: RUMBLORRRR the unfermentable stuck wash

Postby Nathan02 » Sat Jul 28, 2018 7:49 am

roasted goat leg sounds better then stinky billy juice woody :text-lol:
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Re: RUMBLORRRR the unfermentable stuck wash

Postby Doubleuj » Sat Jul 28, 2018 7:53 am

Nathan02 wrote:roasted goat leg sounds better then stinky billy juice woody :text-lol:

:laughing-rolling:
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Re: RUMBLORRRR the unfermentable stuck wash

Postby woodduck » Sat Jul 28, 2018 8:22 am

Ohh it's on the cards, it's a prick of a thing. It jumps and craps on everything. I can't keep the bastard in the paddock.
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Re: RUMBLORRRR the unfermentable stuck wash

Postby EziTasting » Sat Jul 28, 2018 12:12 pm

woodduck wrote:Ohh it's on the cards, it's a prick of a thing. It jumps and craps on everything. I can't keep the bastard in the paddock.


Just take a leg at a time... that’ll fill the dinner table and slow that sucker down!!! :laughing-rolling:
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Re: RUMBLORRRR the unfermentable stuck wash

Postby scythe » Sun Jul 29, 2018 7:51 pm

Sounds like something else took over the wash this time instead of yeast.
pH is dropping so something is working in there.

Chlorine might have killed the initial yeast which allowed what ever is in there now to breed.
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Re: RUMBLORRRR the unfermentable stuck wash

Postby nuddy » Sun Jul 29, 2018 11:01 pm

woodduck I've left the lid off to see let mischief mother nature have a go, might be time to let loose the goat.
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Re: RUMBLORRRR the unfermentable stuck wash

Postby woodduck » Mon Jul 30, 2018 6:41 am

Have ya got a dog? Or a small child even? :laughing-rolling: :laughing-rolling:
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