So I had 2 x TPW that were distilled once, which I watered down to %35 and double distilled them again as I only have a reflux still. I had 11 x 250ml jars, 2 x 300ml, 1 x 1L jar. next time I will hopefully have more of the smaller jars.
I threw the first 400Mls fores away to be sure and was left with about 4L of 92% over the 14 jars. man I struggled to tell the difference between them, I had aired the jars for 24hrs. Was this long enough?
I could definatly smell the very start of heads, very kinda sharp burn your eyes kinda smell / feel. but I really struggled to tell where to cut them. I ended up keep 1.8L @92% for a 4.2L at 40% ( which was more just like ill take the middle of the jars to be sure???) when watered down ( its currently sitting @60% on bourbon staves to age) and the rest is 2.2 L 92% is now just under 5L 40% feints.
I did water down a teaspoon from each jar to try and tell the difference spitting it out and washing the mouth out with water between taste. Im hoping I can start to pick it up better with practise. and maybe not do it after all day in the iron factory