Pure distilling reflux problems
Posted: Sun Mar 08, 2020 9:45 am
We have had this still for years. suddenly it is boiling in the tube, sounds like a train, and vapour is running out the top.
Things we have tried:
Tested the wash it is at lower than 1000
Repacked the column
checked the hole with a needle
Things we have tried:
Tested the wash it is at lower than 1000
Repacked the column
checked the hole with a needle