Hi distillers
This is my first post. I have a Keggomax CM reflux still and 30l electric boiler. My first wash was disappointing- 25l of TPW yielding 2.1l of 89% spirit. Did some reading and increased the packing in the column and put a manifold on the water line to control each water jacket separately. Ran a 27l (TPW )wash last night. Temp stabilized at 79degC. and produced spirit at 91.5%. Was hoping to get higher. As and experiment I took the thermometer of the top of the column, and poured down the column 150ml of the 91.5% spirit. From this I collected 94.5% spirit. Did this with the rest of the spirit to end up with 2.4l of of 94.5% :).
Question 1 My pump delivers only 2.6l/min. Would this be two low a flow rate, and would this be the cause of the poor reflux?
Question 2 Adding distillate to the top of the column gave very good results. Is there a problem with this practise?
Thank you