by Icarus » Tue Dec 20, 2011 10:08 pm
Hi nanna, I have one of these stills and encountered a similiar thing once in a while in the early days of using it.
To fix the cooling water control, I fitted a quater inch brass needle valve from Bearing Service in the cold water inlet supply line between the tap and the still inlet.
These valves give a very fine control of the flow. As I am on a pressure pump from a tank, I had to set up a constant pressure supply as any variation in the pump pressure affected the cooling water flow rate, regardless of control valve setting (a law of hydrodynamics). A flow variation effects the cooling rate and hence the reflux rate in the column.
What was the temperature of your cooling water? I have found that if the cooling water is above 29C, it can cause problems and also if it falls to 20c or lower. It effects the reflux rate in the column as these are CM (Cooling Management) stills.
I have replaced the orignal thermometer with a different, more responsive one and check it against two others I have to confirm it is reading correctly over several temps before I starts a run/runs.
When fitting new genuine packing, you can thourougly wash it and give it a clean with either warm to hot vinegar or citric acid solution first before packing the column. The alternative is to pack the column and then do a cleaning run with the still after fitting the new packing straight from the packet.
When fitting the packing, the first two packing wads should finish level with the bottom of the column water jacket, the third being a looser pack to fill the remainder. Always make sure the packing retainer at the top of the column is in the correct position and that no packing has squeezed past into the condenser outlet vapour space .
Also, overfilling the boiler with wash and not leaving sufficient headspace can heve detrimental effects.
I have found that it works better when the still is cleaned thoroughly after I finsih a run/runs before storing it, especially if it is not going to be used for some time.
Another thing that creates headaches is if there is any unfermented sugar or too much yeast left in the wash.
I am also assuming that your wash had an abv of between 15 and 18% and was fully fermented out.
Hope this helps
cheers, Icarus